Novel approach to control CdS morphology by simple microwave-solvothermal method

Citation

Murugan, A. Vadivel and Kale, B. B. and Kulkarni, Aarti V. and Kunde, Lalita B. and Saaminathan, V. (2005) Novel approach to control CdS morphology by simple microwave-solvothermal method. Journal of Materials Science: Materials in Electronics, 16 (5). pp. 295-299. ISSN 0957-4522

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Abstract

Nanosize CdS powders with different microstructures are prepared in different solvents by using rapid microwave irradiation. Effect of solvents and Cd2+ precursors are to be able to control the particle size, and microstructures of CdS have been investigated by X-ray diffraction and TEM. The different particle size and morphologies are observed using different Cd2+ precursors in different solvents. TEM micrographs clearly show multiarmed nanorods and spherical shape morphologies of CdS powders are obtained in polar solvent like water (H2O), whereas non-polar polyol solvent like ethylene glycol (EG), prickle and cluster like morphologies of CdS are achieved with different Cd2+ precursors such as CdSO4 and Cd (CH3COO)(2). The spectroscopy studies of nanosize CdS are examined by photo-luminescence spectra. Band gap and the absorption co-efficient for nano CdS is also evaluated from optical absorption studies. (C) 2005 Springer Science + Business Media, Inc.

Item Type: Article
Subjects: T Technology > TA Engineering (General). Civil engineering (General)
Divisions: Faculty of Engineering (FOE)
Depositing User: Ms Rosnani Abd Wahab
Date Deposited: 12 Aug 2011 06:43
Last Modified: 12 Aug 2011 06:43
URII: http://shdl.mmu.edu.my/id/eprint/2234

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